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LS 6000 Scintillation System User’s Manual
PN 247971-F
2-8
Getting Started
Using the Racks
racks are supplied if Versa-Rack is installed. Bio-Vial racks are purchased separately and are
used in place of the miniature vial racks.
Each rack has vial position numbers in raised numerals along the bottom edge of one side.
The other side of the rack has two slots, one to hold a Command Card and one to hold a Rack
Number Card. If a Rack Number Card is installed, the Rack Number and position number are
printed next to the Sample Number. Refer to the printouts in Section 5 for an example. The
types of racks and cards are described below.
Standard Racks (White)
These racks hold 12 standard-size vials per rack. A maximum of 28 racks may be loaded at a
time.
Miniature Racks (Blue)
These racks hold 18 miniature vials per rack. A maximum of 36 racks may be loaded at a
time.
Bio-Vial Racks (Green)
These racks hold 18 Bio-Vials. A maximum of 36 racks may be loaded at one time. These
racks can only be used on a system which uses miniature racks.
Color-Coded Racks
A red rack and yellow rack are supplied for use as a HSalt Rack and Interrupt Rack,
respectively. These racks are color coded for easy recognition only; they are identical to the
other standard or miniature racks supplied. If Versa-Rack is installed on your system, the
type of color coded racks matches the size of your unquenched standards. Refer to Section 2
Setting Up the Racks below for information on setting up these racks.
Command Cards
Command Cards have a recognition code (white areas against a black background) which is
“read” by photo sensors. Command Cards are used to instruct the instrument on the
operation to perform; Calibrate, Automatic Count Using A Specific User Number, Auto DPM,
or Halt. Each time a rack bearing one of these cards moves into counting position, the
instrument recognizes the card and takes the appropriate action. The Command Cards can be
stored in a slide out drawer located under the center-front of the instrument. Refer to Section
2 Setting Up the Racks for installing the Command Cards onto the appropriate racks.
Rack Number Cards
Rack Number Cards also have a recognition code (white areas against a black background)
which is “read” by the photo sensors prior to counting samples in the rack during Automatic
Counting. Rack Number Cards are used to indicate the number of the rack providing positive
sample identification. When Rack Number Cards are installed on the sample racks, the
printout shows both rack number and position number within the rack, so a sample can be
located specifically within a batch of samples. Refer to Section 2 Setting Up the Racks for
installing the Rack Number Cards onto the Sample Racks.
- LS 6000 Series 1
- Table of Contents 3
- Introduction 11
- Principles of Operation 12
- Operating the Instrument 12
- Operating Modes 13
- 1.3 Specifications 14
- Precautions and Limitations 15
- Figure 1.1 Standard Vial 15
- Miniature Vials 16
- 1.5 Hazards 17
- Maintenance 18
- Getting Started 19
- 2.2 Power Failure 21
- 2.3 Operating Controls 21
- Operator Control Key pad 22
- Using the Operating Controls 24
- 2.4 Using the Racks 25
- Using the Racks 26
- Setting Up the Racks 27
- 2.5 Preparing the Printer 29
- 2.6 System Setup 30
- Energy Scale 31
- Printer Paging 32
- Allow Interrupt Count 32
- System Setup 33
- Figure 2.9 RS232 Setup Menu 33
- Date/Time 35
- Auto DPM 35
- 2.7 Calibration 36
- Counting Samples 39
- Starting the Automatic Count 40
- Conducting Count Single Rack 41
- 3.4 Auto DPM 46
- 3.5 Multi-Task 47
- Interrupt Count in Multi-Task 48
- Multi-Task 50
- Interrupt Data 51
- Setting Up User Programs 59
- 4.2 Editing A User Program 61
- Editing A User Program 62
- Comments 65
- Counting Time 65
- Liquid or Xtal Scintillator 65
- Isotope 1 65
- Isotope 2 and Isotope 3 66
- Edit Other Parameters 67
- Counting Precision 69
- Background/Blank Subtraction 69
- Lum-Ex Correction 71
- Phase Monitor 72
- Low Level 72
- Low Count Reject 72
- Output Formats 72
- Count Data 75
- Raw Data 75
- Collecting Spectral Data 76
- 4.3 Copy User Program 77
- Copy User Program 78
- 5.2 CPM/Xtal CPM 80
- CPM/Xtal CPM 81
- Results for CPM/Xtal CPM 83
- 5.4 Auto DPM 85
- Setting Up Auto DPM 86
- Loading Samples for Auto DPM 86
- Results for Auto DPM 86
- Setting Up DPM 87
- 5.6 Xtal DPM 89
- Xtal DPM 90
- Setting Up Xtal DPM 91
- Loading Samples for Xtal DPM 92
- 5.7 DPM % of Reference 93
- Setting Up DPM % of Reference 94
- Xtal SL DPM % of Reference 95
- 5.9 Single Photon Monitoring 98
- Data Calculation 100
- Single Photon Monitoring 100
- Isotope/DPM Libraries 103
- Accessing the Isotope Library 104
- Printing the Isotope Library 104
- The Isotope Library 105
- Setup Menu 106
- PN 247971-F 108
- 5 minutes 109
- 6.2 Setting Up A Quench Curve 110
- Setting Up A Quench Curve 112
- Counting the Standards 114
- Editing Quench Curves 120
- Deleting A Quench Curve 124
- Manual Entry of Quench Curves 125
- 7.1 Chemiluminescence 127
- Interpretation of Results 128
- Reducing Single Photon Events 128
- 7.3 Two Phase Samples 129
- Procedures 131
- Analysis of Data 131
- H Counting Efficiency 132
- C Counting Efficiency 132
- Background 133
- Contamination 133
- Instrument Specifications 135
- Temperature Control Accessory 138
- Installation Requirements 139
- Electrical Requirements 140
- 0.5 to 1.0 m in 140
- Environment Requirements 142
- . Note that the output 144
- Datum IDs 146
- CHAPTER 1, PART 31 167
- Region I 170
- Region II 170
- Region III 170
- Region IV 170
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